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Three details to note in vacuum heat treatment of experimental vacuum furnace

The vacuum tempering furnace should have a quick cooling device. The pressure of cooling water should be greater than 0.2Mpa, the flow rate should be adjustable. Heating up: after putting in the workpiece, generally pre-pumping to 6.67Pa before heating up the heating process, the workpiece and the furnace material will be deflated, so that the vacuum level drops. Cooling gas: generally use 99.995% purity of nitrogen, high temperature alloys using 99.999% nitrogen or argon, titanium alloys using 99.995% argon. Vacuum furnace active connection part all use O-ring sealing connection, this part are through water cooling. Vacuum annealing, vacuum annealing, vacuum solution treatment and vacuum aging heating temperature is generally the same as the heating temperature of conventional treatment. Workpiece quenching under vacuum, should use vacuum quenching oil, this oil has a low saturated vapor pressure. Vacuum furnace maintenance should be in a vacuum or pure nitrogen state, to avoid the usual use of air absorption, moisture absorption. Domestic vacuum furnace pressure rise rate should not be greater than 1.33 Pa / h, the standard of some foreign companies for 0.67 Pa / h vacuum furnace treatment of titanium alloys, should not use nitrogen as a cooling gas, because titanium and nitrogen at high temperature reaction, the formation of golden yellow titanium nitride. The vacuum heating is based on radiation, and the workpiece should be kept spaced in the furnace.

Jun 06,2016

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